Calcium acetate monohydrate → Calcium Acetate

HRID 1439155Notes

Reaction equation

HRID 1439155 reaction equation
O.[C:2]([O-:5])(=[O:4])[CH3:3].[Ca+2:6].[C:7]([O-:10])(=[O:9])[CH3:8]>C(O)CO>[C:2]([O-:5])(=[O:4])[CH3:3].[Ca+2:6].[C:7]([O-:10])(=[O:9])[CH3:8]

Participants

3

Reactant 1

HCID 82163Calcium acetate monohydrate

Product 1

HCID 6116Calcium Acetate

Reagents, catalysts & solvents 1

HCID 174Ethylene GlycolSolvent2×

Procedure

A tank located within a circulating circuit of a homogenizer was charged with 30 Kg of ethylene glycol and 1.22 Kg or calcium acetate monohydrate, and these materials were homogenized at room temperature for 45 minutes. Then, the mixture was transferred into a catalyst preparing tank held at 40° C., and stirred for 3 hours to form a solution of calcium acetate in ethylene glycol.

Workup

  1. customThen, the mixture was transferred into a catalyst preparing tank
  2. customheld at 40° C.
  3. stirringstirred for 3 hours

Sources & evidence

ORD record
ord-660df6508f124ca1b297b3f0b83c4212
Source dataset
uspto-grants-1977_11
Patent number
US04058507

Reaction notes

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