HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → N-Methyl-N-(2-methyl-1,3-dichloro-2-propanesulfenyl)carbamoyl fluoride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | 3-Chloro-2-methyl-1-propene | HCID 11241 | — |
| Reactant | N-chlorothio(methyl)carbamoyl fluoride | HCID 12922862 | — |
| Product | N-Methyl-N-(2-methyl-1,3-dichloro-2-propanesulfenyl)carbamoyl fluoride | HCID 54204012 | — |
Reaction Steps
To a solution of 1.35g of methallyl chloride in 25 ml of methylene chloride was added 2.15g of N-methyl-N-chlorosulfenyl carbamoyl fluoride. The solution was heated to reflux for 45 min. and concentrated to 1.68g of pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04058549 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-d9e055816b2943b28be3fc34bc7e884f |
| Source note | uspto-grants-1977_11 |