Hydrochloric Acid → HCID 13019381, compound

HRID 1439285Notes

Reaction equation

HRID 1439285 reaction equation
[CH2:1]([NH:17][C:18]1[CH:31]=[CH:30][C:21]([C:22]([O:24][CH2:25][CH:26]([OH:29])[CH2:27][OH:28])=[O:23])=[CH:20][CH:19]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[ClH:32]>C(Cl)(Cl)(Cl)Cl>[ClH:32].[CH2:1]([NH:17][C:18]1[CH:19]=[CH:20][C:21]([C:22]([O:24][CH2:25][CH:26]([OH:29])[CH2:27][OH:28])=[O:23])=[CH:30][CH:31]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 130193802,3-Dihydroxypropyl 4-(n-hexadecylamino)benzoate

Product 1

HCID 13019381HCID 13019381, compound

Reagents, catalysts & solvents 1

HCID 5943Carbon TetrachlorideSolvent

Procedure

A solution of 15.0 g of 2,3-dihydroxypropyl 4-(n-hexadecylamino)benzoate in 700 ml of carbon tetrachloride is stirred under reflux and is treated with anhydrous hydrogen chloride. The mixture is allowed to cool and is filtered to yield 2,3-dihydroxypropyl 4-(n-hexadecylamino)benzoate hydrochloride as a white solid, mp 126°-130° C.

Workup

  1. temperatureunder reflux
  2. temperatureto cool
  3. filtrationis filtered

Sources & evidence

ORD record
ord-3f2af034146c4a72910eb3eb76d8817f
Source dataset
uspto-grants-1977_11
Patent number
US04058550

Reaction notes

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