HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 2770500, compound → (+-)-Tetramisole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 2770500 | HCID 2770500 | — |
| Solvent | Sodium Carbonate | HCID 10340 | — |
| Product | (+-)-Tetramisole | HCID 3913 | — |
Reaction Steps
Method A ##STR90## 2-Imino-3-(2'-chloro-2'-phenylethyl)thiazolidine hydrochloride (27.7 g) was heated for 1 hour on a steam-bath with 200 ml of 2N sodium carbonate solution. During this time an oil formed. On cooling this solidified. It was separated and recrystallised from 20% aq. ethanol to yield the desired compound. The hydrochloride was obtained by dissolving the base in ethanol and saturating the solution with dry HCl.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04059588 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-3ff1da8b24694b359577ed5dd8b87187 |
| Source note | uspto-grants-1977_11 |