HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 20338676, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 21395750 | HCID 21395750 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 20338676 | HCID 20338676 | — |
Reaction Steps
1-(2-Hydroxypropyl)-4-phenylpiperazine hydrochloride (155 g.) was suspended in 1200 ml. dry chloroform and 87.5 ml. thionyl chloride added dropwise. The mixture was refluxed 21/2 hrs, and cooled overnight at room temperature. The solid was filtered, washed with chloroform, them with ether, and dried to give 175 g., m. 216-18° .
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04060526 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-863c2927b9114ffabeb6d501c11a1baf |
| Source note | uspto-grants-1977_11 |