HCID 86735224, compound → HCID 86735223, compound

Participants

Reaction Steps

trans-3-Ethyl-dl-prolineamide hydrochloride (0.5 g) was dissolved in water and passed down a column of DEAE-Sephadex resin (OH- form). The fractions containing product (as detected by t.l.c.) were combined and evaporated to dryness to yield trans-3-ethyl-dl-prolineamide hydrate (0.45 g) as a white solid m.p. 89.5°-91° RF 3A 0.22 RF 3B 0.72

Provenance & Evidence