HCID 21396264, compound → HCID 21396260, compound

Participants

Reaction Steps

Silver acetate (3.34 g) was added with cooling and stirring to a solution of 2-(2-benzoyloxyethoxy)ethoxymethyl chloride (5.18 g) in dry acetonitrile (15 ml). The reaction mixture was stirred overnight at room temperature. The precipitate was removed by filtration and the filtrated evaporated under reduced pressure at 35° C. to give 2-(2-benzoyloxyethoxy)ethoxymethyl acetate (5.5 g) as a pale yellow oil. NMR and IR spectra were consistent with this structure.

Provenance & Evidence