HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Pyridin-2-yl)butan-1-amine → HCID 178512150, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Pyridin-2-yl)butan-1-amine | HCID 13511083 | — |
| Reactant | N-Nitro-S-methylisothiourea | HCID 135927615 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178512150 | HCID 178512150 | — |
Reaction Steps
A solution of 2-(4-aminobutyl)pyridine (2.9 g) and S-methyl-N-nitroisothiourea (2.9 g) in methanol (50 ml) was heated at 50-65° for 4-5 hours. Concentration, followed by recrystallisation of the residue yielded N-[4-(2-pyridyl)butyl]-N'-nitroguanidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04060621 |
| Source dataset | uspto-grants-1977_11 |
| ORD ID | ord-a8c2b2ddd9164ec193eb1ff0e98dd278 |
| Source note | uspto-grants-1977_11 |