Phenylacetaldehyde → HCID 11171585, compound

HRID 1439759Notes

Reaction equation

[C:1]1([CH2:7][CH:8]=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C1(CCC=O)C=CC=CC=1.[Cl:20][CH2:21][CH2:22][CH2:23]I.ClCCI>>[Cl:20][CH2:21][CH2:22][CH2:23][C:8](=[O:9])[CH2:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

Reactant 4

HCID 998Phenylacetaldehyde

HCID 7707Benzenepropanal

HCID 813631-Chloro-3-iodopropane

HCID 1364381-Chloro-2-iodoethane

Product 1

HCID 11171585HCID 11171585, compound

Procedure

When in the procedure of Example 2 0.10 mole of phenylacetaldehyde is substituted for 3-phenylpropionaldehyde, and 0.10 mole of 1-chloro-3-iodopropane is substituted for 1-chloro-2-iodoethane, 5-chloro-1-phenylpentan-2-one is obtained.

Sources & evidence

ORD record: ord-7896b088b16344d19cc325afd081aa00
Source dataset: uspto-grants-1977_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04060630

Reaction notes

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