Iodoethane → HCID 21396404, compound

HRID 1439763Notes

Reaction equation

HRID 1439763 reaction equation
[NH2:1][CH2:2][CH2:3][N:4]([CH2:13][C:14]([C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)=[O:15])[C:5]1[CH:10]=[C:9]([Cl:11])[CH:8]=[CH:7][C:6]=1[Cl:12].Cl[C:23]1C=CC(Cl)=C[C:24]=1NCCN(CC)CC.C(I)C.ClCC(C1C=CC=CC=1)=O>>[CH2:23]([NH:1][CH2:2][CH2:3][N:4]([CH2:13][C:14]([C:16]1[CH:17]=[CH:18][CH:19]=[CH:20][CH:21]=1)=[O:15])[C:5]1[CH:10]=[C:9]([Cl:11])[CH:8]=[CH:7][C:6]=1[Cl:12])[CH3:24]

Participants

5

Reactant 4

HCID 6340IodoethaneHCID 107572-ChloroacetophenoneHCID 21396386HCID 21396386, compoundHCID 21396401HCID 21396401, compound

Product 1

HCID 21396404HCID 21396404, compound

Procedure

When in the procedure of Example 5 an appropriate amount of 2-[N-(β-aminoethyl)-N-(2,5-dichlorophenyl)amino]acetophenone is substituted for N-(2,5-dichlorophenyl)-N',N'-diethylethylenediamine and an appropriate amount of ethyliodide is substituted for 2-chloroacetophenone, 2-[N-(β-ethylaminoethyl)-N-(2,5-dichlorophenyl)amino]acetophenone is obtained.

Sources & evidence

ORD record
ord-1d522738867948dfad7647bca507b422
Source dataset
uspto-grants-1977_11
Patent number
US04060630

Reaction notes

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