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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1439828Generated: November 1, 2026

HCID 53828474, compound → HCID 14766834, compound

https://huagongshe.com/reaction/1439828

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 53828474HCID 53828474—
CatalystPalladiumHCID 23938—
SolventTetrahydrofuranHCID 8028—
ProductHCID 14766834HCID 14766834—

Reaction Steps

A solution of 10.6 g of 1-(p-n-propylphenyl)-2-(4'-fluorobiphenyl-4-yl)ethene [obtained by Heck coupling of 4-propylstyrene with 4-bromo-4'-n-fluorobiphenyl] in 200 ml of tetrahydrofuran is hydrogenated in the presence of Pd/C until the take-up H of is complete. Customary work-up gives 1-(p-propylphenyl)-2-(4'-fluorobiphenyl-4-yl)ethane, mp. 97°.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05496499
Source datasetuspto-grants-1996_03
ORD IDord-c81b1e84946848fe8b664e73e91ea2fc
Source noteuspto-grants-1996_03