Triethylamine → HCID 54566527, compound

HRID 1439961Notes

Reaction equation

HRID 1439961 reaction equation
[C:1]([O:8][CH:9]1[CH2:14][C:13]([CH3:16])([CH3:15])[NH:12][C:11]([CH3:18])([CH3:17])[CH2:10]1)(=[O:7])[CH2:2][CH2:3][C:4]([O-:6])=[O:5].Br[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH3:31].C(N(CC)CC)C>>[C:4]([O:6][CH2:31][CH2:30][CH2:29][CH2:28][CH2:27][CH2:26][CH2:25][CH2:24][CH2:23][CH2:22][CH2:21][CH3:20])(=[O:5])[CH2:3][CH2:2][C:1]([O:8][CH:9]1[CH2:14][C:13]([CH3:16])([CH3:15])[NH:12][C:11]([CH3:18])([CH3:17])[CH2:10]1)=[O:7]

Participants

4

Reactant 3

HCID 8471TriethylamineHCID 89191-BromododecaneHCID 86749308HCID 86749308, compound

Product 1

HCID 54566527HCID 54566527, compound

Procedure

The product is prepared as described in Example 4b by reacting 30.9 g (0.12 mol) of mono(2,2,6,6-tetramethyl-4-piperidyl) succinate with 29.9 g (0.12 mol) of 1-bromododecane in the presence of 12.1 g (0.12 mol) of triethylamine. The product obtained has a boiling point of 195° C./5.3 mbar.

Workup

  1. customThe product is prepared
  2. customThe product obtained

Sources & evidence

ORD record
ord-0ac7b96db76343c78136c912f4c63af4
Source dataset
uspto-grants-1996_03
Patent number
US05496875

Reaction notes

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