Triethylamine → HCID 53808655, compound

HRID 1439962Notes

Reaction equation

HRID 1439962 reaction equation
[C:1]([O:8][CH:9]1[CH2:14][C:13]([CH3:16])([CH3:15])[N:12]([CH3:17])[C:11]([CH3:19])([CH3:18])[CH2:10]1)(=[O:7])[CH2:2][CH2:3][C:4]([O-:6])=[O:5].Br[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32].C(N(CC)CC)C>>[C:4]([O:6][CH2:32][CH2:31][CH2:30][CH2:29][CH2:28][CH2:27][CH2:26][CH2:25][CH2:24][CH2:23][CH2:22][CH3:21])(=[O:5])[CH2:3][CH2:2][C:1]([O:8][CH:9]1[CH2:14][C:13]([CH3:15])([CH3:16])[N:12]([CH3:17])[C:11]([CH3:19])([CH3:18])[CH2:10]1)=[O:7]

Participants

4

Reactant 3

HCID 8471TriethylamineHCID 89191-BromododecaneHCID 85850356HCID 85850356, compound

Product 1

HCID 53808655HCID 53808655, compound

Procedure

The product is prepared as described in Example 4b by reacting 27.1 g (0.1 mol) of mono(1,2,2,6,6-pentamethyl-4-piperidyl) succinate with 24.9 g (0.1 mol) of 1-bromododecane in the presence of 10.1 g (0.1 mol) of triethylamine. The product has a boiling point of 190° C./4 mbar.

Workup

  1. customThe product is prepared

Sources & evidence

ORD record
ord-2b0ddcc1352848219c5c118c58d6973e
Source dataset
uspto-grants-1996_03
Patent number
US05496875

Reaction notes

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