L-Phenylalanine → HCID 22859211, compound

HRID 1440065Notes

Reaction equation

HRID 1440065 reaction equation
[NH2:1][C@H:2]([C:10]([OH:12])=[O:11])[CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[C:13]([S:16][CH2:17][CH:18]([CH3:22])[C:19](Cl)=[O:20])(=[O:15])[CH3:14]>>[C:13]([S:16][CH2:17][CH:18]([CH3:22])[C:19]([NH:1][C@H:2]([C:10]([OH:12])=[O:11])[CH2:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)=[O:20])(=[O:15])[CH3:14]

Participants

3

Reactant 2

HCID 6140L-PhenylalanineHCID 103458Ethanethioic acid, S-(3-chloro-2-methyl-3-oxopropyl) ester

Product 1

HCID 22859211HCID 22859211, compound

Procedure

Following the procedure of Example 16, L-phenylalanine is reacted with 3-acetylthio-2-methylpropanoyl chloride to give (±)-N-[3-(acetylthio)-2-methyl-1-oxopropyl]-L-phenylalanine.

Sources & evidence

ORD record
ord-af48b9aa6a2e4ea390343576764dd6ff
Source dataset
uspto-grants-1996_03
Patent number
US05496805

Reaction notes

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