HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21995488, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 18970394 | HCID 18970394 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21995488 | HCID 21995488 | — |
Reaction Steps
To 30 ml of methanol saturated with hydrogen chloride gas was added 9.72 g of N,N'-di-t-butoxycarbonyl-2,8-diazabicyclo[4.3.0]non-5-ene, stirred at room temperature for 4 hours, and then evaporated under reduced pressure to obtain 5.85 g of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05498615 |
| Source dataset | uspto-grants-1996_03 |
| ORD ID | ord-f8a5bf962d1f43af9b6c74eae19b9134 |
| Source note | uspto-grants-1996_03 |