Hydrochloric Acid → HCID 21995488, compound

HRID 1440210Notes

Reaction equation

HRID 1440210 reaction equation
[ClH:1].C(OC([N:9]1[CH2:17][CH:16]2[C:11](=[CH:12][CH2:13][CH2:14][N:15]2C(OC(C)(C)C)=O)[CH2:10]1)=O)(C)(C)C>CO>[ClH:1].[ClH:1].[CH:16]12[CH2:17][NH:9][CH2:10][C:11]1=[CH:12][CH2:13][CH2:14][NH:15]2

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 18970394HCID 18970394, compound

Product 1

HCID 21995488HCID 21995488, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

To 30 ml of methanol saturated with hydrogen chloride gas was added 9.72 g of N,N'-di-t-butoxycarbonyl-2,8-diazabicyclo[4.3.0]non-5-ene, stirred at room temperature for 4 hours, and then evaporated under reduced pressure to obtain 5.85 g of the desired compound.

Workup

  1. customevaporated under reduced pressure

Sources & evidence

ORD record
ord-f8a5bf962d1f43af9b6c74eae19b9134
Source dataset
uspto-grants-1996_03
Patent number
US05498615

Reaction notes

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