HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → 4,5-Dihydroxy-2-nitrobenzeneacetonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | Cyclohexene | HCID 8079 | — |
| Reactant | [4,5-Bis(benzyloxy)-2-nitrophenyl]acetonitrile | HCID 10904838 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4,5-Dihydroxy-2-nitrobenzeneacetonitrile | HCID 10921393 | — |
Reaction Steps
0.75 g of palladium at a concentration of 10% on charcoal, to which 3 g of charcoal have been added, followed by 0.02 mole (7.5 g) of 2-nitro-4,5-dibenzyloxyphenylacetonitrile, are added with stirring to 30 ml of 96° C. ethanol containing 15 ml of cyclohexene; the reaction mixture is heated under reflux for 1 hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05498746 |
| Source dataset | uspto-grants-1996_03 |
| ORD ID | ord-4899053939e24cce8d7e8c75e621e982 |
| Source note | uspto-grants-1996_03 |