HRID1440441

反应详情

EQUATION

反应方程式

HRID 1440441 的结构方程式

PROCEDURE

实验过程

Using 3-hydroxy-4-methylbenzoic acid (20.3 g, 0.13 mole)and benzyl chloride (50.8 g, 0.40 mole), the reaction was carried out in the same manner as described in Example 1, (1). The resulting crude solid was recrystallized from ethanol to give 15.0 g of 3-benzyloxy-4-methylbenzoic acid as white crystals having a m.p. of 159°-161° C.

WORKUP

后处理

  1. customThe resulting crude solid was recrystallized from ethanol