HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → 3-(Benzyloxy)-4-methylbenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | 3-Hydroxy-4-methylbenzoic acid | HCID 68512 | — |
| Reactant | 1,2,10-Tris(4-hydroxybenzoyloxy)anthracene | HCID 22903228 | — |
| Product | 3-(Benzyloxy)-4-methylbenzoic acid | HCID 22903188 | 47.6% |
Reaction Steps
Using 3-hydroxy-4-methylbenzoic acid (20.3 g, 0.13 mole)and benzyl chloride (50.8 g, 0.40 mole), the reaction was carried out in the same manner as described in Example 1, (1). The resulting crude solid was recrystallized from ethanol to give 15.0 g of 3-benzyloxy-4-methylbenzoic acid as white crystals having a m.p. of 159°-161° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05498748 |
| Source dataset | uspto-grants-1996_03 |
| ORD ID | ord-441a136a29cc419c9e20887733b38b81 |
| Source note | uspto-grants-1996_03 |