o-Xylyl bromide → Dimethyl [(2-methylphenyl)methyl]phosphonate

HRID 1440667Notes

Reaction equation

[CH3:1][C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[CH2:4]Br.[CH3:10][O:11][P:12]([O:15]C)[O:13][CH3:14]>>[CH3:1][C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[CH2:4][P:12](=[O:15])([O:13][CH3:14])[O:11][CH3:10]

Participants

Reactant 2

HCID 6992o-Xylyl bromide

HCID 8472Trimethyl phosphite

Product 1

HCID 2773780Dimethyl [(2-methylphenyl)methyl]phosphonate

Procedure

Following the procedure of Compound 11, 2-methylbenzyl bromide is reacted with trimethylphosphite.

Sources & evidence

ORD record: ord-d97942920dcc4d869fcbe9de43cff26e
Source dataset: uspto-grants-1996_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05500417

Reaction notes

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