p-Xylyl bromide → Dimethyl [(4-methylphenyl)methyl]phosphonate

HRID 1440669Notes

Reaction equation

[CH3:1][C:2]1[CH:9]=[CH:8][C:5]([CH2:6]Br)=[CH:4][CH:3]=1.[CH3:10][O:11][P:12]([O:15]C)[O:13][CH3:14]>>[CH3:1][C:2]1[CH:9]=[CH:8][C:5]([CH2:6][P:12](=[O:15])([O:13][CH3:14])[O:11][CH3:10])=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 7721p-Xylyl bromide

HCID 8472Trimethyl phosphite

Product 1

HCID 2773783Dimethyl [(4-methylphenyl)methyl]phosphonate

Procedure

Following the procedure of Compound 11, 4-methylbenzyl bromide is reacted with trimethylphosphite.

Sources & evidence

ORD record: ord-9db3edcd3774454d8cf2ba4b47de7f88
Source dataset: uspto-grants-1996_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05500417

Reaction notes

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