1-Butanol → Benzoyl Peroxide

Participants

Reaction Steps

In a flask was charged 450 parts of n-butanol, and a mixture of 240 parts of styrene, 180 parts of 2-ethylhexyl acrylate, 300 parts of methyl acrylate, 500 parts of the epoxy resin-bound acrylic monomer solution obtained in Synthesis example 19 and 15 parts of benzoyl peroxide was gradually added dropwise at 80° to 90° C. over 3 hours. Then, a mixture of 2 parts of benzoyl peroxide and 30 parts of n-butanol was gradually added dropwise at the same temperature over 30 minutes. Stirring was continued for further 2 hours at the same temperature to obtain an epoxy resin-bound acrylic resin solution having a solid component of 60%.

Provenance & Evidence