1-Butanol → Benzoyl Peroxide

HRID 1440837Notes

Reaction equation

HRID 1440837 reaction equation
[CH2:1]=[CH:2][C:3]1[CH:8]=CC=CC=1.C([O:13][CH2:14][CH:15]([CH2:20][CH3:21])[CH2:16][CH2:17][CH2:18]C)(=O)C=C.[C:22]([O:26]C)(=[O:25])[CH:23]=[CH2:24].C([OH:32])CCC>>[C:22]([O:26][O:32][C:14](=[O:13])[C:15]1[CH:16]=[CH:17][CH:18]=[CH:21][CH:20]=1)(=[O:25])[C:23]1[CH:8]=[CH:3][CH:2]=[CH:1][CH:24]=1

Participants

5

Reactant 4

HCID 2631-ButanolHCID 7294Methyl AcrylateHCID 7501StyreneHCID 76362-Ethylhexyl acrylate

Product 1

HCID 7187Benzoyl Peroxide

Procedure

In a flask was charged 450 parts of n-butanol, and a mixture of 240 parts of styrene, 180 parts of 2-ethylhexyl acrylate, 300 parts of methyl acrylate, 500 parts of the epoxy resin-bound acrylic monomer solution obtained in Synthesis example 19 and 15 parts of benzoyl peroxide was gradually added dropwise at 80° to 90° C. over 3 hours. Then, a mixture of 2 parts of benzoyl peroxide and 30 parts of n-butanol was gradually added dropwise at the same temperature over 30 minutes. Stirring was continued for further 2 hours at the same temperature to obtain an epoxy resin-bound acrylic resin solution having a solid component of 60%.

Sources & evidence

ORD record
ord-08a908cb74484b9a8a1ecbe32bf740dc
Source dataset
uspto-grants-1996_03
Patent number
US05500463

Reaction notes

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