HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18982548, compound → HCID 18982489, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18982548 | HCID 18982548 | — |
| Reactant | HCID 23668465 | HCID 23668465 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18982489 | HCID 18982489 | 93.1% |
Reaction Steps
An aqueous solution of 11.27 g of lithium butyltriphenylborate in 200 ml of water was added to an aqueous solution of 8.21 g of dimethyl-p-chlorobenzylsulfonium chloride in 200 ml of water, and the resultant mixture was stirred at room temperature for 30 minutes. Then, the reaction mixture was filtered, and the resultant crystal was washed with water and dried to give 16.67 g of dimethyl-p-chlorobenzylsulfonium-butyltriphenylborate as a white crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05500453 |
| Source dataset | uspto-grants-1996_03 |
| ORD ID | ord-d19b8ba586f840c1961acd4be2ceb9c7 |
| Source note | uspto-grants-1996_03 |