Methanol → HCID 18982492, compound

Participants

Reaction Steps

A solution of 2.80 g of lithium methyl-tris(p-fluorophenyl)borate in 50 ml of acetonitrile was added to a solution of 5.00 g of bis(p-chlorophenyl)(p-methoxyphenacyl)sulfonium hexafluorophosphate in 100 ml of acetonitrile, and the resultant mixture was stirred at room temperature for 30 minutes. Then, 200 ml of methanol was added. The resultant precipitate of a crystal was recovered, and 100 ml of dichloromethane was added. The dichloromethane layer was washed with water, dried and concentrated to give 3.31 of bis(p-chlorophenyl)-(p-methoxyphenacyl)sulfonium-methyl-tris(p-fluorophenyl)borate.

Provenance & Evidence