Water → HCID 88398096, compound

Participants

Reaction Steps

A solution of 5.58 g of lithium (2-tert-butylethenyl)tris(p-bromophenyl)borate in 50 ml of acetonitrile was added to a solution of 6.41 g of phenyl(1-naphthyl)(1-naphthyl-carbonylmethyl)sulfonium hexafluoroantimonate in 100 ml of acetonitrile, and the resultant mixture was stirred at room temperature for 30 minutes. Then, 200 ml of water was added. The resultant precipitate of a yellow oily component was recovered, and 100 ml of dichloromethane was added. The dichloromethane layer was washed with water, dried and concentrated to give 4.27 of phenyl(1-naphthyl)(1-naphthyl-carbonylmethyl)sulfonium-(2-tert-butylethenyl)tris(p-bromophenyl)borate.

Provenance & Evidence