Water → HCID 88398164, compound

Participants

Reaction Steps

A solution of 5.59 g of sodium (2-tert-butylethenyl)trimesitylborate in 50 ml of acetone was added to a solution of 5.00 g of diphenyl-p-fluorophenacylsulfonium perchlorate in 100 ml of acetonitrile, and the resultant mixture was stirred at room temperature for 30 minutes. Then, 200 ml of water was added. The resultant precipitate of a yellow oily component was recovered, and 100 ml of dichloromethane was added. The dichloromethane layer was washed with water, dried and concentrated to give 3.11 of diphenyl-p-fluorophenacylsulfonium-(2-tert-butylethenyl)trimesitylborate.

Provenance & Evidence