HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 54426322, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 22859581 | HCID 22859581 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 54426322 | HCID 54426322 | — |
Reaction Steps
5-(5-Methoxycarbonyl-2-furyl)-3-(1-methylpyrrolidin-2(R)-ylmethyl)-1H-indole (see Example 65) was reacted with lithium aluminium hydride, in tetrahydrofuran, using a procedure similar to that described in Example 63. This gave the title compound. Found: C,70.59; H,6.81; N,8.41. C19H22N2O2.3/16CH2Cl2 requires: C,70.62; H,6.91; N,8.59%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05502065 |
| Source dataset | uspto-grants-1996_03 |
| ORD ID | ord-f37bdcd1d2b94eb3a10cac1c894b9216 |
| Source note | uspto-grants-1996_03 |