HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68542475, compound → HCID 23088194, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68542475 | HCID 68542475 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23088194 | HCID 23088194 | 80.8% |
Reaction Steps
To a solution of 2-benzyloxy-4,6-dimethylpyridin-3-yl 3-fluoro-4-methylphenyl methanol (0.39 g) in ethanol (10 mL) was added a catalytic amount of palladium carbon powder, and the mixture was stirred at room temperature under a hydrogen atmosphere overnight. After the insoluble material was removed by filtration, the solvent of the filtrate was removed to give the title compound (0.22 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07655633B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-73fb2390e4c742809d25e66043eac5a8 |
| Source note | uspto-grants-2010_02 |