HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 44591734, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178522752 | HCID 178522752 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 44591734 | HCID 44591734 | — |
Reaction Steps
2,4-Dichloro-N-[4-(cyclopropylmethyl)-1-(1H-[1,2,3]triazole-4-sulfonyl)piperidin-4-ylmethyl]benzamide (472 mg, 1.0 mmol) was dissolved in N,N-dimethylformamide (5 mL). Potassium carbonate (276 mg, 2 mmol) and methyl iodide (81 μL, 1.3 mmol) were added and the mixture stirred at room temperature over night.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07655644B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-74357077942943cdbbbbc0e3ce23eaf7 |
| Source note | uspto-grants-2010_02 |