HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68689654, compound → HCID 69385700, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68689654 | HCID 68689654 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69385700 | HCID 69385700 | 105.3% |
Reaction Steps
4-[N-(Propionyl)-N-(isopropyl)amino]-5-methylisoxazole (Method 6; 330 g, 1.0 eq.) was stirred under hydrogen (1.0 eq), with 10% palladium on carbon (0.1 eq.) in EtOH (10 vol.eq.) at 25° C. overnight. The catalyst was removed by filtration and the EtOH was removed in vacuo to leave an off white solid (351 g, 98%). This was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07655652B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-c79c5cfb24eb4020bac32dd704953c85 |
| Source note | uspto-grants-2010_02 |