HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitromethane → 25963-52-4
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitromethane | HCID 6375 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 178420937 | HCID 178420937 | — |
| Product | 25963-52-4 | HCID 13563696 | — |
Reaction Steps
A mixture of nitromethane and carbon bisulfide dissolved in alcohols is added dropwise to the solution of potassium hydroxide in alcohol at room temperature. The reaction is carried out at the temperature range of 0-35° C. for 2-10 hours. The solid is filtered out to afford a crude product potassium 2-nitroethene-1,1-bis(thiolate) which is a brown yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07655665B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-49af9c59a3674e97bbe0909755d6ffb4 |
| Source note | uspto-grants-2010_02 |