HRID1441731

反应详情

EQUATION

反应方程式

HRID 1441731 反应方程式

AUXILIARIES

试剂、催化剂与溶剂

3

PROCEDURE

实验过程

A solution of compound 50B (200 mg, 1.298 mmol) and 10% Pd/C (˜5 mg) in MeOH and AcOH was stirred under H2 at 1 atmosphere for 30 minutes. The reaction solution was filtered through a pad of celite eluting with MeOH. The MeOH was removed under reduced pressure to give compound 50C.

WORKUP

后处理

  1. filtrationThe reaction solution was filtered through a pad of celite
  2. washeluting with MeOH
  3. customThe MeOH was removed under reduced pressure