Benzyl Bromide → HCID 19995077, compound

HRID 1441959Notes

Reaction equation

HRID 1441959 reaction equation
[OH:1][C:2]1[CH:3]=[C:4]([CH:7]=[C:8]([OH:10])[CH:9]=1)[CH:5]=[O:6].[CH2:11](Br)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1.C(=O)([O-])[O-].[Cs+].[Cs+]>>[CH2:11]([O:1][C:2]1[CH:3]=[C:4]([CH:7]=[C:8]([OH:10])[CH:9]=1)[CH:5]=[O:6])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

4

Reactant 3

HCID 7498Benzyl BromideHCID 10796Cesium carbonateHCID 943653,5-Dihydroxybenzaldehyde

Product 1

HCID 19995077HCID 19995077, compound

Procedure

Preparation takes place in analogy to Example 3H from 5.0 g (36.2 mmol) of 3,5-dihydroxybenzaldehyde, 6.81 g (39.8 mmol) of benzyl bromide and 11.8 g (36.2 mmol) of cesium carbonate.

Workup

  1. customPreparation

Sources & evidence

ORD record
ord-2e3e31e6558d4443be1e65496ea4db2c
Source dataset
uspto-grants-2010_02
Patent number
US07655643B2

Reaction notes

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