HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 9903389, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Isophthalonitrile | HCID 12276 | — |
| Reactant | Benzoic acid, 2-mercapto-, methyl ester | HCID 21009 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 9903389 | HCID 9903389 | 3.4% |
Reaction Steps
A mixture of isophthalonitrile (1.00 g, 07.8 mmol), methyl thiosalicylate (1.97 g, 12 mmol), triethylamine (1.34 g, 13 mmol) and toluene (5 ml) was heated and refluxed for 5 hours under a nitrogen flow. The precipitated crystals were taken by filtration and recrystallized from tetrahydrofuran-ethanol to give the title compound (0.07 g, 2%) as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07659267B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-55720152173f46a7b04ab0e854420e03 |
| Source note | uspto-grants-2010_02 |