HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59166707, compound → HCID 59166716, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59166707 | HCID 59166707 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 59166716 | HCID 59166716 | 80.4% |
Reaction Steps
2-[1-(4-Benzyloxy-3-methyl-phenyl)-1-ethyl-propyl]-benzooxazole-5-carboxylic acid methyl ester (3.28 g, 7.39 mmol) and Pd—C (300 mg, 10%) is hydrogenated analogous to Example 1, step F to give the title product (2.10 g, 80%). MS (ES) m/e: 354.2 (M+1), 352.2 (M−1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07659296B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-3692db25ddb949cd84c55a53e046385d |
| Source note | uspto-grants-2010_02 |