HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86628006, compound → HCID 18442652, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86628006 | HCID 86628006 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 18442652 | HCID 18442652 | — |
Reaction Steps
A solution of tert-butyl [3-(cyclopropylmethyl)-2-oxo-4-phenyl-2,3-dihydro-1H-imidazol-1-yl]acetate from Step C (41 mg, 0.125 mmol) in CH2Cl2 (2 mL) and CF3CO2H (1 mL) was stirred at ambient temperature for 3 h. The mixture was concentrated in vacuo to afford the title compound. MS: m/z=273 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07659300B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-a26f9f60f4da4ae78cc9aa3f41c4f874 |
| Source note | uspto-grants-2010_02 |