HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 76593241, compound → HCID 75290666, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 76593241 | HCID 76593241 | — |
| Solvent | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Product | HCID 75290666 | HCID 75290666 | 38.5% |
Reaction Steps
Compound 103 (75 mg, 0.09 mmol) was stirred for 2 h in a mixture of dichloro-methane-trifluoroacetic acid; 2:1. Evaporation and purification by HPLC gave pure title compound (25 mg, 38%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07659245B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-b647e9d53b9047c68eaa580deec57e19 |
| Source note | uspto-grants-2010_02 |