HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 68786969, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 4-Amino-4'-cyanobiphenyl | HCID 97193 | — |
| Reactant | 4-Bromobutanol | HCID 118388 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 68786969 | HCID 68786969 | — |
Reaction Steps
4′-amino-(1,1′-Biphenyl)-4-carbonitrile is dissolved in dimethyl formamide. Sodium hydride is added to the solution followed by 4-bromo-1-hydroxybutane to provide 4′-(4-hydroxybutylamino)-(1,1′-Biphenyl)-4-carbonitrile. 4′-(4-hydroxybutylamino)-(1,1′-Biphenyl)-4-carbonitrile is suspended in dichloromethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662572B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-33d0127aafd44e1a8c151baec86d18ff |
| Source note | uspto-grants-2010_02 |