HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67442555, compound → HCID 67441600, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67442555 | HCID 67442555 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67441600 | HCID 67441600 | — |
Reaction Steps
A mixture of 4-(4-nitrophenyl)-1,4-diaza-bicyclo[3.2.2]nonane (0.50 g, 2.0 mmol), palladium on carbon (100 mg, 10%) and methanol (60 ml) was stirred for 15 minutes under hydrogen (130 ml of hydrogen was consumed). The crude mixture was filtered through celite and the product was isolated as an oil in quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662808B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-9ab75ab9fbbd4a4989d928ef965e6db2 |
| Source note | uspto-grants-2010_02 |