HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexanoyl chloride → HCID 25005968, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexanoyl chloride | HCID 67340 | — |
| Reactant | HCID 44248849 | HCID 44248849 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 25005968 | HCID 25005968 | 82.7% |
Reaction Steps
Following the procedure in Example 1, Step 4, 5,6,9,10,11,12-hexahydro-4H,8H-cyclohepta[4,5]pyrrolo[3,2,1-ij]quinolin-2-amine (0.12 g, 0.50 mmol), hexanoyl chloride (0.072 mL, 0.52 mmol) and poly-(4-vinylpyridine) (700 mg) in dichloromethane (10 mL) provided 0.14 g of N-5,6,9,10,11,12-hexahydro-4H,8H-cyclohepta[4,5]pyrrolo[3,2,1-ij]quinolin-2-ylhexanamide. MS (ESI) m/z 339;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662831B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-8986d583c960497783d635159911f64b |
| Source note | uspto-grants-2010_02 |