HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 13464813, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Cyclooctanone | HCID 10403 | — |
| Reactant | 2,3-dihydro-1H-indol-1-amine | HCID 2760932 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13464813 | HCID 13464813 | 30.7% |
Reaction Steps
Following the procedure of Example 1, Step 1, cyclooctanone (6.9 mL, 52 mmol), 1-aminoindoline (7.0 g, 52 mmol) and concentrated sulfuric acid (10 mL) in water (90 mL) provided 4,5,7,8,9,10,11,12-octahydrocycloocta[b]pyrrolo[3,2,1-hi]indole (3.6 g). MS (ES) m/z 226.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662831B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-233689e7d7db444993ebfa1bed81a00f |
| Source note | uspto-grants-2010_02 |