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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1444013Generated: November 4, 2026

Hydrochloric Acid → HCID 59168137, compound

https://huagongshe.com/reaction/1444013

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantLithium hydroxide, monohydrateHCID 168937—
ReactantHCID 59168168HCID 59168168—
SolventMethanolHCID 887—
SolventWaterHCID 962—
ProductHCID 59168137HCID 59168137—

Reaction Steps

A mixture of 3-[6-chloro-3-(2,3-dichlorobenzenesulphonylamino)-2-pyrazinyloxymethyl]benzoic acid methyl ester (Example 104) (0.3 g) and lithium hydroxide hydrate (0.2 g) in water (5 mL) and methanol (5 mL) was stirred at room temperature. After 3 h, hydrochloric acid (2M) was added to acidify the mixture and the solid product was collected by filtration and dried (0.25 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07662825B2
Source datasetuspto-grants-2010_02
ORD IDord-d63b9bdd8e3649aa8a31f80acdef4f70
Source noteuspto-grants-2010_02