HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-3-chloropyrazine → HCID 59168216, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-3-chloropyrazine | HCID 276224 | — |
| Reactant | 3-Methoxybenzenesulfonyl chloride | HCID 2737504 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59168216 | HCID 59168216 | — |
Reaction Steps
By the method outlined in Example 1 (reaction performed at room temperature) using 3-chloro-2-aminopyrazine (0.83 g), 3-methoxybenzenesulfonyl chloride (1.44 g). The crude adduct was reacted with a solution of sodium methoxide (10 mL of a 25% solution in methanol) in methanol (20 mL) to afford the sub-titled compound (1.41 g) as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662825B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-4e6f1fc170524a31980cc36840a76069 |
| Source note | uspto-grants-2010_02 |