HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-((Dimethylamino)methyl)-2-furanmethanol → HCID 10174871, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-((Dimethylamino)methyl)-2-furanmethanol | HCID 84906 | — |
| Reactant | 2,3-Dichloro-N-(3,5-dibromo-2-pyrazinyl)benzenesulphonamide | HCID 59168219 | — |
| Product | HCID 10174871 | HCID 10174871 | — |
Reaction Steps
Prepared by the method of Example 31 using (5-dimethylaminomethyl-2-furanyl)methanol (0.2 g) and 2,3-dichloro-N-(3,5-dibromo-2-pyrazinyl)benzenesulphonamide (Example 31a) (0.2 g). Purified by silica gel chromatography eluting with methanol/dichloromethane mixtures and recrystallised from acetonitrile. Yield 0.058 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662825B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-d471efd7ba9a41aea37e39681ecd510d |
| Source note | uspto-grants-2010_02 |