HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-[(Methylamino)methyl]-2-furanmethanol → 2,3-Dichloro-N-[3-(5-methylaminomethyl-2-furanylmethoxy)-2-pyrazinyl]benzenesulphonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-[(Methylamino)methyl]-2-furanmethanol | HCID 14671747 | — |
| Reactant | 2,3-Dichloro-N-(3-chloro-2-pyrazinyl)benzenesulphonamide | HCID 59168167 | — |
| Product | 2,3-Dichloro-N-[3-(5-methylaminomethyl-2-furanylmethoxy)-2-pyrazinyl]benzenesulphonamide | HCID 59168112 | — |
Reaction Steps
Prepared by the method of Example 28 using (5-methylaminomethyl-2-furanyl)methanol (0.2 g) and 2,3-dichloro-N-(3-chloro-2-pyrazinyl)benzenesulphonamide (Example 28) (0.4 g). Purified by silica gel chromatography eluting with methanol/dichloromethane mixtures. Yield 0.12 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662825B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-80c3591449d748149af6acb2f226633a |
| Source note | uspto-grants-2010_02 |