HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propargyl alcohol → HCID 10309050, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propargyl alcohol | HCID 7859 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 2,3-Dichloro-N-(3-chloro-2-pyrazinyl)benzenesulphonamide | HCID 59168167 | — |
| Product | HCID 10309050 | HCID 10309050 | — |
Reaction Steps
Prepared by the method of Example 28 using propargyl alcohol as solvent (3 mL), 2,3-dichloro-N-(3-chloro-2-pyrazinyl)benzenesulphonamide (Example 28) (0.3 g) and sodium hydride (0.2 g of a 60% dispersion in oil) at room temperature for 16 h. Yield 0.27 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662825B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-cbaaebce16204488855405321111808b |
| Source note | uspto-grants-2010_02 |