HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → N-Benzylidene(piperidin-4-yl)methanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | 4-(Aminomethyl)piperidine | HCID 23527 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | N-Benzylidene(piperidin-4-yl)methanamine | HCID 11820173 | — |
Reaction Steps
Benzaldehyde (4.6 g; 0.044 mol) was added dropwise to a solution of 4-aminomethylpiperidine (5.0 g; 0.044 mol) in toluene (20 ml). The solution thus obtained was stirred for 3 h at room temperature. Then the solvent was removed by evaporation at reduced pressure and the residue was taken up twice with toluene to give the desired product that was used as such without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662836B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-5924d5348ad944b5b28619e072e9943f |
| Source note | uspto-grants-2010_02 |