HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminocinnamic acid ethyl ester → Ethyl 3-[3-[[[6-(3,5-dichlorophenyl)-2-pyridinyl]carbonyl]amino]phenyl]-2-propenoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminocinnamic acid ethyl ester | HCID 97825 | — |
| Reactant | HCID 24730153 | HCID 24730153 | — |
| Product | Ethyl 3-[3-[[[6-(3,5-dichlorophenyl)-2-pyridinyl]carbonyl]amino]phenyl]-2-propenoate | HCID 68499249 | — |
Reaction Steps
Carboxylic acid (131) (50 mg, 0.19 mmol) was coupled to aniline (60) (40 mg, 0.21 mmol) using Method D. The residue was triturated with TBME (3 ml) to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07662839B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-23ae165dfeaa4d40b89b5dfebd02e76e |
| Source note | uspto-grants-2010_02 |