HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diphenylacetylene → Dibenzyl
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diphenylacetylene | HCID 10390 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Dibenzyl | HCID 7647 | 100% |
Reaction Steps
In Example 5, hydrogenation reaction was conducted under the same condition as Example 1 for THF diluted solution concentration of the substance to be reduced, its flow rate, and hydrogen 9 flow rate, using 1,2-diphenylacetylene as the substance to be reduced. The reaction time was within five minutes. The analytical result of the reaction product by 1H-NMR showed almost complete hydrogenation of 1,2-diphenylacetylene, and 1,2-diphenylethane was obtained at about 100% yield (See FIG. 6.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07663008B2 |
| Source dataset | uspto-grants-2010_02 |
| ORD ID | ord-0450aa5b9c794ff78c106cf3010b2794 |
| Source note | uspto-grants-2010_02 |